By K. Bode, I. Kuriyama, J.E. Mark, F. Maser, M. Mutter, Y. Nakose, A. Odajima, V.N.R. Pillai, J.P. Queslel, H.W. Siesler
With contributions through various specialists
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Apart from a general intensity decrease as a consequence of the reduction in sample thickness the intensities of the 1459/1455 cm -1 bands (not resolved here) of the crystalline at-modification drastically decrease while the intensity of the 1475/1470 cm -1 band complex exhibits a relative increase. This result can be attributed to the predominant formation of a fibrillar structure with the abovementioned imperfect all-trans conformation of the aliphatic segments. Once the neck has completely moved across the specimen (at about 350 ~ strain) stress increases linearly with strain.
Siesler has first reported the application of rapid-scanning F T t R spectroscopy to monitor the spectral changes in small time intervals during elongation, recovery and stressrelaxation of PTMT films 7, t62-165) The film samples utilized for the rheo-optical studies were prepared from PTMT chips by hot pressing at 523 K and quenching in ice water. Sections of this sample were drawn in hot water to a draw ratio of ~. = 4 and finally annealed at constant length under vacuum at 483 K for 15 hours.
43). From these results it can be concluded that in the crystalline phase the molecular orientation is completed almost immediately after elongation, while in the amorphous phase the polymer chains are further oriented during the fast decay region of stressrelaxation. These findings are in good agreement with previously reported results of rheo-optical IR orientation measurements of natural rubber 2o3) and suggest that the stress-relaxation can be primarily ascribed to the amorphous rather than the crystalline orientation.
Analysis, Networks, Peptides by K. Bode, I. Kuriyama, J.E. Mark, F. Maser, M. Mutter, Y. Nakose, A. Odajima, V.N.R. Pillai, J.P. Queslel, H.W. Siesler